HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54342320, compound → 2-butyl-6-methylpyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54342320 | HCID 54342320 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-butyl-6-methylpyridine | HCID 219541 | 92.5% |
Reaction Steps
The picoline from Step 1 (970 mg) was hydrogenated for 50 minutes at 20 psi of hydrogen in EtOAc (30 mL) using 5% Pd/C (90 mg) as catalyst. Filtration and concentration in vacuo gave 910 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506227 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-868a8e5470cd43d6bd2a89818b392288 |
| Source note | uspto-grants-1996_04 |