HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3,4-Dichlorophenoxy)acetic acid → HCID 18603269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3,4-Dichlorophenoxy)acetic acid | HCID 11495 | — |
| Reactant | Cyclohexanamine, N-methyl-2-(1-pyrrolidinyl)-, trans- | HCID 13377463 | — |
| Product | HCID 18603269 | HCID 18603269 | — |
Reaction Steps
The title compound was prepared according to the method described in Example 2, using 3,4-dichlorophenoxyacetic acid (2.34 g, 11 mmol) and (±)-trans-N-methyl-N-[2-(1-pyrrolidinyl)cyclohexyl]amine prepared in Example 1 (2 g, 11 mmol). The crude product, which started to precipitate before the addition of the diethyl ether, was recrystallised from hot dichloromethane. Yield 2.9 g (62%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506257 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-f450219564a54cf28b79e61e172337c4 |
| Source note | uspto-grants-1996_04 |