(3,4-Dichlorophenoxy)acetic acid → HCID 22860081, compound

Participants

Reaction Steps

The title compound was prepared according to the method described in Example 2, using 3,4-dichlorophenoxyacetic acid (2.51 g, 11 mmol), and (±)-trans-N-methyl-N-[2-(4-morpholinyl)cyclohexyl]amine prepared in Example 12 (2 g, 10 mmol). The crude product, which precipitated without the addition of any diethyl ether, was recrystallised from hot methanol. Yield 3.42 g (78%). Proton and carbon-13 NMR data in accord.

Provenance & Evidence