HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphonoacetate → HCID 22418304, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphonoacetate | HCID 13345 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 3-Methoxybenzyl chloride | HCID 69994 | — |
| Product | HCID 22418304 | HCID 22418304 | 76% |
Reaction Steps
By working in a way similar to that described in example 11 and by using ethyl diethoxyphosphinylacetate (59 g; 0.26 moles), sodium hydride at 60% (9.33 g; 0.233 moles) and 3-methoxybenzyl chloride (20.62 g; 0.13 moles), ethyl 2-diethoxyphosphinyl-3-(3-methoxyphenyl)-propionate (34 g; 76% yield) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506259 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-11048b8c8f924e14901ff109cb462182 |
| Source note | uspto-grants-1996_04 |