HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54035213, compound → L-Proline, 1-(1-oxo-4-phenylbutyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54035213 | HCID 54035213 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | L-Proline, 1-(1-oxo-4-phenylbutyl)- | HCID 10355295 | 90.4% |
Reaction Steps
To N-(4-phenylbutyryl)-L-proline benzyl ester (9.31 g) in 99% methanol (100 ml) was added 10% Pd--C (0.90 g), and the mixture was stirred at room temperature in hydrogen stream for 2 hours. The catalyst was filtered off with celite, and the filtrate was concentrated to give 6.26 g of N-(4-phenylbutyryl)-L-proline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506256 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-093d4f60198c4cb49e25d28aeb7c5dc6 |
| Source note | uspto-grants-1996_04 |