HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2S)-1-(N-Benzylaminocarbonyl-L-prolyl)-2-(1-hydroxy-2-phenoxyethyl)pyrrolidine → HCID 57059660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2S)-1-(N-Benzylaminocarbonyl-L-prolyl)-2-(1-hydroxy-2-phenoxyethyl)pyrrolidine | HCID 57230620 | — |
| Reactant | Dmso dcc | HCID 86749402 | — |
| Product | HCID 57059660 | HCID 57059660 | 53.8% |
Reaction Steps
(2S)-1-(N-Benzylaminocarbonyl-L-prolyl)-2-(1-hydroxy-2-phenoxyethyl)pyrrolidine (798 mg) was subjected to DMSO-DCC oxidation as in Example 1D), followed by recrystallization from ethyl acetate-hexane to give 427 mg of the title compound (See Table 6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506256 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-ea02a28b7d764a5ba1be6732bf751c5b |
| Source note | uspto-grants-1996_04 |