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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1720516Generated: October 31, 2026

Diphosgene → HCID 67771423, compound

https://huagongshe.com/reaction/1720516

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiphosgeneHCID 10426—
Reactant4-FluorobenzylamineHCID 67326—
ReactantHCID 67771616HCID 67771616—
ProductHCID 67771423HCID 67771423—

Reaction Steps

By the same procedure as in Example 28-B), while using 4-fluorobenzylamine (0.54 ml), trichloromethyl chloroformate (0.28 ml) and (2S)-1-[N-(tert-butoxycarbonyl)-L-prolyl]-2-[2-(4-fluorophenoxy)-1-hydroxyethyl]pyrrolidine (1.85 g), there was obtained 1.38 g of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05506256
Source datasetuspto-grants-1996_04
ORD IDord-2750883772fa4033a81a965f7d4fdac4
Source noteuspto-grants-1996_04