HRID1720519

反应详情

EQUATION

反应方程式

HRID 1720519 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of N-octanoyl-L-proline benzyl ester (7.04 g) in 1% water-containing methanol (70 ml) was added 10% Pd-C (0.71 g), and the mixutre was stirred under hydrogen atmosphere at room temperature for 1.5 hours. After the catalyst was filtered off, the filtrate was concentrated to give 5.08 g of the title compound.

WORKUP

后处理

  1. filtrationAfter the catalyst was filtered off
  2. concentrationthe filtrate was concentrated