HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[(1-Adamantyl)methoxycarbonyl]-L-proline benzyl ester → HCID 49760536, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[(1-Adamantyl)methoxycarbonyl]-L-proline benzyl ester | HCID 53719614 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 49760536 | HCID 49760536 | 99.9% |
Reaction Steps
To a solution of N-[(1-adamantyl)methoxycarbonyl]-L-proline benzyl ester (1.98 g) in methanol (60 ml) was added 10% Pd-C (0.20 g), and the mixture was stirred at room temperature under hydrogen atmosphere for 1.5 hours. The catalyst was filtered off, and the filtrate was concentrated to give 1.53 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506256 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-ca786530c6f64b82afbce9a09d1f922f |
| Source note | uspto-grants-1996_04 |