Allyl Alcohol → HCID 57258425, compound

HRID 1720541Notes

Reaction equation

HRID 1720541 reaction equation
[CH2:1]([OH:4])[CH:2]=[CH2:3].[CH3:5][O:6][CH:7]([O:10][CH3:11])[CH2:8]Br>>[CH3:5][O:6][CH:7]([O:10][CH3:11])[CH2:8][O:4][CH2:1][CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 7858Allyl AlcoholHCID 816722-Bromo-1,1-dimethoxyethane

Product 1

HCID 57258425HCID 57258425, compound

Procedure

Perkin Elmer 8310 GC (8% carbowax+2% KOH on chromasorb 80-100 mesh, 80°-200° C. in 20 min. Product retention 5.775 minutes, allyl alcohol 3.61 min, bromo-acetaldehyde dimethyl acetal 5.44 min. FID detection.

Sources & evidence

ORD record
ord-ebbbf1ce42534b029206f1f32aea1309
Source dataset
uspto-grants-1996_04
Patent number
US05506345

Reaction notes

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