Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-(2,5-Dimethylphenoxymethyl)-alpha-methoxyiminophenylacetic acid | HCID 54397424 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54157125 | HCID 54157125 | — |
Reaction Steps
Toluene (10 ml), thionyl chloride (1.36 g, 11 mmol) and dimethylformamide (DMF) (0.1 ml) were added to the crude 2-[2-(2,5-dimethylphenoxymethyl)phenyl]-2-methoxyiminoacetic acid (Z=at least 99%)(2.99 g, 9.5 mmol), and the mixture was stirred at 70° C. for 1.5 hours. After completion of the reaction, the mixture was concentrated to give crude 2-[2-(2,5-dimethylphenoxymethyl)phenyl]-2-methoxyiminoacetyl chloride (E/Z=75/25).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05506358 |
|---|
| Source dataset | uspto-grants-1996_04 |
|---|
| ORD ID | ord-9a4ad7a7d56442debed8869bd11ce76c |
|---|
| Source note | uspto-grants-1996_04 |
|---|
