HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57238962, compound → HCID 22844604, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57238962 | HCID 57238962 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22844604 | HCID 22844604 | 100.3% |
Reaction Steps
44 mg of (4S,5RS)-3-benzyloxycarbonyl-4-cyclohexylmethyl-2,2-dimethyl-5-[(1RS)-1-hydroxy-2-(2-methoxyethylamino)ethyl]oxazolidine was dissolved in 1.5 ml of ethanol, and palladium black was added thereto. The mixture was treated in the same manner as in Example 17 to obtain 27 mg of (2RS,3RS,4S)-4-amino-5-cyclohexyl-1-(2-methoxyethylamino)-2,3-pentanediol as colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506356 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-6407972b5f344e30b39cacc25210f6db |
| Source note | uspto-grants-1996_04 |