HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57141636, compound → HCID 22844606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57141636 | HCID 57141636 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22844606 | HCID 22844606 | 109.9% |
Reaction Steps
44 mg of (4S,5RS)-3-benzyloxycarbonyl-4-cyclohexylmethyl-2,2-dimethyl-5-[(1RS)-1-hydroxy-2-(diethylamino)ethyl]oxazolidine was dissolved in 1.5 ml of ethanol, and palladium black was added thereto. The mixture was treated in the same manner as in Example 17 to obtain 29.5 mg of (2RS,3RS,4S)-4-amino-5-cyclohexyl-1-diethylamino-2,3-pentanediol as colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506356 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-e774da4172804897b014cf31aca967d1 |
| Source note | uspto-grants-1996_04 |