HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86749436, compound → HCID 54266952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86749436 | HCID 86749436 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 54266952 | HCID 54266952 | 100% |
Reaction Steps
A solution of 4-(N-(2-((2R)-2,3-bis(palmitoyloxy)propylthio)-ethylsulfonyl)-N-t-butyloxycarbonylaminomethyl)benzoyl -glutamic acid de-t-butyl ester as obtained in Example 56 (108 mg) in trifiuoroacetic acid (1 ml) was stirred at room temperature for 1 hour, followed by concentration to dryness under reduced pressure, to yield the title compound (89 mg, yield 100%) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506267 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-ee9da90854dd44aba50fce749b946bdb |
| Source note | uspto-grants-1996_04 |