HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroform → HCID 22416306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Bromide | HCID 253877 | — |
| Reactant | Toluene ethylacetate | HCID 21584019 | — |
| Reactant | HCID 22416310 | HCID 22416310 | — |
| Product | HCID 22416306 | HCID 22416306 | — |
Reaction Steps
IR (KBr): ν=3037 cm-1, 2918, 2850, 1608, 1596, 1519, 1441, 1290, 1264, 1257, 833, 787. -UV (CH3CN), qual.: λmax =301 mn, 370 (sh). - UV (CHCl3): λmax (log ε)=303 nm (4.325), 330 (sh, 4.201), 370 (sh, 3.234). - 1H NMR (CDCl3): δ=1.15-1.45 (m, 35H, OCH2C17H35) , 3.97 (t, 2H, OCH2C17H35), 7.01 (d, 2H, CCHCHCOC18H37), 7.54 (d, 2H, CCHCHCOC18H37), 8.47 (d, 2H, NCHCH), 8.74 (d, 2H, NCHCH), 9.00 (s, 2H, pyrimidine-H). -MS (70 eV): m/z (%)=501 (61) [M+ ], 249 (100) . - TLC (CH2Cl2 /methanol 1/1): Rf =0.65.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05507974 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-21ccb80bc8cd4248a6359a1421167c4a |
| Source note | uspto-grants-1996_04 |