HCID 22417130, compound → HCID 22417170, compound

HRID 1721101Notes

Reaction equation

HRID 1721101 reaction equation
[C:1]([O:5][C:6]([N:8]1[CH2:12][CH:11]([CH2:13][OH:14])[C:10]2([CH2:18][CH2:17][CH2:16]C2)[CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].C(OC(N1CC(CO)C2(CCCCC2)C1)=O)(C)(C)C>>[C:1]([O:5][C:6]([N:8]1[CH2:12][CH:11]([CH2:13][OH:14])[C:10]2([CH2:16][CH2:17][CH2:18]2)[CH2:9]1)=[O:7])([CH3:3])([CH3:4])[CH3:2]

Participants

3

Reactant 2

HCID 22417130HCID 22417130, compound2×HCID 22417224HCID 22417224, compound2×

Product 1

HCID 22417170HCID 22417170, compound

Procedure

In the similar procedure, 2-tert-butoxycarbonyl-4-hydroxymethyl-2-azaspiro[4.4]nonane (compound 105) (1H-NMR (CDCl3) δppm: 1.46 (9H, s), 1.61 (8H, s), 3.0-3.9 (7H, m)) and 2-tert-butoxycarbonyl-4-hydroxymethyl-2-azaspiro[4.5]decane (compound 107)

Sources & evidence

ORD record
ord-53e5a200d3be462c89e82a99bfb0c6ee
Source dataset
uspto-grants-1996_04
Patent number
US05508428

Reaction notes

Loading…