HCID 135966859, compound → HCID 136082986, compound

Participants

Reaction Steps

To a solution of 0.48 g 5-benzyloxy-indole-3-carboxaldehyde amino(N-methyl-N-heptylamino)methylene hydrazone (1.1 mmol) in EtOH there is added 0.25 g 10% Pd/C. The suspension is hydrogenated overnight at 45° C. Afterwards the suspension is filtered over silica gel, the solvent is evaporated and the residue is chromatographed over silica gel (eluant:toluene/EtOH/NH3 85:15:1) to yield the title compound. The pure material is crystallized from CH2Cl2 /Hexane 2: 8.

Provenance & Evidence