4-(Phenylmethyl)phenyl diethylcarbamate → 2-(1-Oxo-5-phenoxypentyl)-4-(phenylmethyl)phenyl diethylcarbamate

HRID 1721382Notes

Reaction equation

HRID 1721382 reaction equation
[CH2:1]([N:3]([CH2:20][CH3:21])[C:4](=[O:19])[O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:8][CH:7]=1)[CH3:2].CON(C)[C:25](=[O:37])[CH2:26][CH2:27][CH2:28][CH2:29][O:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1>>[CH2:20]([N:3]([CH2:1][CH3:2])[C:4](=[O:19])[O:5][C:6]1[CH:11]=[CH:10][C:9]([CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)=[CH:8][C:7]=1[C:25](=[O:37])[CH2:26][CH2:27][CH2:28][CH2:29][O:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1)[CH3:21]

Participants

3

Reactant 2

HCID 224149984-(Phenylmethyl)phenyl diethylcarbamateHCID 22415008N-methoxy-N-methyl-5-phenoxypentanamide

Product 1

HCID 538545992-(1-Oxo-5-phenoxypentyl)-4-(phenylmethyl)phenyl diethylcarbamate

Procedure

The title compound was prepared from 4-(phenylmethyl)phenyl diethylcarbamate and N-methoxy-N-methyl-5-phenoxypentanamide following the same procedure used in Example F. NMR (CDCl3) δ1.18 (t, 3H), 1.26 (t, 3H), 1.83 (m, 4H), 2.92 (t, 2H), 3.35 (q, 2H), 3.45 (q, 2H) 3.99 (m, 4H), 6.86-7.31 (m, 12H), 7.49 (d, 1H).

Sources & evidence

ORD record
ord-f1ecce7a2c694ef58dad4d9d5baeb7ca
Source dataset
uspto-grants-1996_04
Patent number
US05510375

Reaction notes

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