Ethanol → Ethyl sulfoacetate

HRID 1721388Notes

Reaction equation

HRID 1721388 reaction equation
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

Participants

3

Reactant 2

HCID 702EthanolHCID 31257Sulfoacetic acid

Product 1

HCID 12216623Ethyl sulfoacetate

Procedure

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

Workup

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

Sources & evidence

ORD record
ord-25099fe8278a4bf3ab4105d4b60c77d8
Source dataset
uspto-grants-1996_04
Patent number
US05510379

Reaction notes

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