HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86749452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 86749453 | HCID 86749453 | — |
| Product | HCID 86749452 | HCID 86749452 | — |
Reaction Steps
2,6-Diisopropylphenoxysulfonyl acetic acid (prepared as described in Example 3) was reacted with oxalyl chloride to provide 2,6-diisopropylphenoxysulfonyl acetyl chloride. The acid chloride was reacted with 2,6-diisopropylphenol in dichloromethane to provide, following evaporation of the reaction solvent, 2,6-diisopropylphenyl (2,6-diisopropylphenoxycarbonyl)methyl sulfonate, mp 90°-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05510379 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-9d08456b1260486fa422431015eced5b |
| Source note | uspto-grants-1996_04 |