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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1721939Generated: October 29, 2026

Allyl bromide → HCID 14622792, compound

https://huagongshe.com/reaction/1721939

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAllyl bromideHCID 7841—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 15631674HCID 15631674—
SolventAcetoneHCID 180—
ProductHCID 14622792HCID 1462279287.2%

Reaction Steps

A suspension of 8.35 g of 2,3-dichloro-4-(1-methyl-5-pyrazolylcarbonyl)phenol, 5.59 g of allyl bromide and 10.64 g of potassium carbonate in acetone is refluxed for 3 hours. The reaction mixture is filtered and the filtrate is evaporated to remove solvent. The residue is dissolved in toluene, and the solution is treated with activated charcoal and then evaporated to give 8.36 g of (2,3-dichloro-4-allyloxyphenyl)(1-methyl-5-pyrazolyl)methanone.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04853404
Source datasetuspto-grants-1989_08
ORD IDord-825abbebcc0d433ba54c60ebf6d6b3fa
Source noteuspto-grants-1989_08