HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → HCID 14622792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 15631674 | HCID 15631674 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14622792 | HCID 14622792 | 87.2% |
Reaction Steps
A suspension of 8.35 g of 2,3-dichloro-4-(1-methyl-5-pyrazolylcarbonyl)phenol, 5.59 g of allyl bromide and 10.64 g of potassium carbonate in acetone is refluxed for 3 hours. The reaction mixture is filtered and the filtrate is evaporated to remove solvent. The residue is dissolved in toluene, and the solution is treated with activated charcoal and then evaporated to give 8.36 g of (2,3-dichloro-4-allyloxyphenyl)(1-methyl-5-pyrazolyl)methanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853404 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-825abbebcc0d433ba54c60ebf6d6b3fa |
| Source note | uspto-grants-1989_08 |