HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178519861, compound → HCID 178519860, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178519861 | HCID 178519861 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178519860 | HCID 178519860 | 94% |
Reaction Steps
A suspension of 4 (5 g, 0.018 mol), EtOH (250 ml) and 10% Pd/C (1.7 g) was hydrogenated on a Parr shaker at 50 psi. After shaking overnight, the suspension was filtered under N2 through a super cel pad. The solution was concentrated to dryness to yield 3.2 g (94%) of 5. An analytical sample was prepared by crystallization from CH3CN; m.p. 212°-214° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853383 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-ea005c9b966c4fdbbb8c2b4006ebfc08 |
| Source note | uspto-grants-1989_08 |