Hydrochloric Acid → HCID 178515903, compound

Participants

Reaction Steps

Into a glass, thick-walled tube was placed 11 (1.5 g, 0.0063 mol) and 12N HCl (100 ml). The contents were frozen and the tube sealed and placed in a bath at 120° C. After 5 days, the contents in the tube were cooled, filtered, the solid stirred overnight with saturated NaHCO3 solution and filtered to yield 0.59 g (49%) of 13.

Provenance & Evidence