HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178494801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 178478453 | HCID 178478453 | — |
| Product | HCID 178494801 | HCID 178494801 | 94% |
Reaction Steps
Under N2, Na (0.7 g, 0.029 mol) was added to CH3OH (100 ml) and heated at reflux. After the Na had reacted, a solution of 70 (2.0 g, 0.0064 mol) in CH3OH (75 ml) was added dropwise with stirring. After 15 hours, the suspension was concentrated to dryness to yield 1.85 g (94%) of 71, m.p. 154°-6° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853383 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-4ec4e69966ad467795d4bdb1d9fa8862 |
| Source note | uspto-grants-1989_08 |