2-Iodothiophene → HCID 9989594, compound

HRID 1722242Notes

Reaction equation

C(O)CCC#C.IC1SC=CC=1.[S:13]1[CH:17]=[CH:16][CH:15]=[C:14]1[C:18]#[C:19][CH2:20][CH2:21][CH:22]=[O:23]>>[S:13]1[CH:17]=[CH:16][CH:15]=[C:14]1[C:18]#[C:19][CH2:20][CH2:21][CH2:22][OH:23]

Participants

Reactant 3

HCID 189212-Iodothiophene

HCID 793464-Pentyn-1-ol

HCID 544425635-Thienyl-4-pentyn-1-al

Product 1

HCID 9989594HCID 9989594, compound

Procedure

5-thienyl-4-pentyn-1-ol was prepared from 4-pentyn-1-ol and 2-iodothiophene as in Example 15 and converted into 5-thienyl-4-pentyn-1-al as in Example 9.

Sources & evidence

ORD record: ord-5c1f092353234b6abd030f6630f8be46
Source dataset: uspto-grants-1989_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04855086

Reaction notes

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