Phosphorus tribromide → HCID 56635606, compound

HRID 1722256Notes

Reaction equation

HRID 1722256 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[CH2:12][CH2:13][CH2:14][CH:15]([CH2:22]O)[C:16]=3[C:17]=2[C:18]=1[CH2:19][O:20][CH3:21])=[O:5])[CH3:2].P(Br)(Br)[Br:25]>ClCCl>[CH2:1]([O:3][C:4]([C:6]1[N:7]=[CH:8][C:9]2[NH:10][C:11]3[CH2:12][CH2:13][CH2:14][CH:15]([CH2:22][Br:25])[C:16]=3[C:17]=2[C:18]=1[CH2:19][O:20][CH3:21])=[O:5])[CH3:2]

Participants

4

Reactant 2

HCID 24614Phosphorus tribromideHCID 54128041HCID 54128041, compound

Product 1

HCID 56635606HCID 56635606, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

From 5,6,7,8-tetrahydro-5-hydroxymethyl-4-methoxymethyl-beta-carboline-3-carboxylic acid ethyl ester (example 2) by reaction with phosphorus tribromide in dichloromethane.

Sources & evidence

ORD record
ord-302a56c0db9d476b8eb7c0395e508d1d
Source dataset
uspto-grants-1989_08
Patent number
US04855295

Reaction notes

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