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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1722432Generated: November 1, 2026

Methyl p-toluenesulfonate → HCID 20028813, compound

https://huagongshe.com/reaction/1722432

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl p-toluenesulfonateHCID 6645—
ReactantHCID 14548451HCID 14548451—
ProductHCID 20028813HCID 20028813—

Reaction Conditions

Temperature130 °C

Reaction Steps

A mixture of 9.46 g (2.5×10-2 mol) of 3,5-dicarbomethoxyphenyldiphenylphosphine (from Preparation 4), and 4.66 g (2.5×10-2 mol) of methyl p-toluenesulfonate was heated in a 130° C. bath with nitrogen bubbling through the melt for two hours. The resultant product was cooled to an amorphous glass.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04855396
Source datasetuspto-grants-1989_08
ORD IDord-2b6dad58e7e74b49ad15fc12ad10a07c
Source noteuspto-grants-1989_08