Methyl iodide → HCID 12772315, compound

HRID 1722563Notes

Reaction equation

HRID 1722563 reaction equation
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][N:3]=1.[CH3:9][I:10]>>[I-:10].[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][N+:3]=1[CH3:9]

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 5818662-Amino-4-chloropyridine

Product 1

HCID 12772315HCID 12772315, compound

Procedure

The starting material was obtained by allowing a mixture of 2-amino-4-chloropyridine and excess methyl iodide (no solvent) to stand at ambient temperature for 2 days to give 2-amino-4-chloro-1-methylpyridinium iodide as a solid, n.m.r. in d6DMSO:-3.6(s, 3H); 6.6-6.7(m, 1H); 7.0(d, 1H); 7.9(d, 1H).

Workup

  1. customThe starting material was obtained

Sources & evidence

ORD record
ord-1ce93554c7474fe3bb90ffc310130307
Source dataset
uspto-grants-1989_08
Patent number
US04855420

Reaction notes

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