HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → Benzenemethanamine, 3,5-dichloro-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 178526342 | HCID 178526342 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Benzenemethanamine, 3,5-dichloro- | HCID 457602 | 70% |
Reaction Steps
The reaction of 3,5-dichlorobenzaldehyde methoxime, (17.4 g, 85.7 mmole) and 0.98M borane in tetrahydrofuran (86 ml) substantially as described in 1B above produced 10.5 g (70%) of the title compound as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857540 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-78c3969df7534f67ae6bc3e3c2e1fb48 |
| Source note | uspto-grants-1989_08 |