HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-nitrobenzene → N-benzyl-2-nitroaniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-nitrobenzene | HCID 6945 | — |
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | N-benzyl-2-nitroaniline | HCID 521800 | 98% |
Reaction Steps
Reaction of 2-chloronitrobenzene (10 g, 63 mmole), benzylamine (40 g, 380 mmole) and ammonium acetate (4.6 g) substantially as described in 1C above produced 14 g (98%) of title compound as orange crystals: mp 65°-67°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857540 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-6cc7eb345d4448edbe81fee62f11ce88 |
| Source note | uspto-grants-1989_08 |