Furan → HCID 20027406, compound

HRID 1722746Notes

Reaction equation

HRID 1722746 reaction equation
C[Si]([O:5][C:6]1[C:11]([Cl:12])=[CH:10][C:9](I)=[CH:8][C:7]=1[Cl:14])(C)C.[O:15]1[CH:19]=[CH:18][CH:17]=[CH:16]1>>[Cl:14][C:7]1[CH:8]=[C:9]([C:16]2[O:15][CH:19]=[CH:18][CH:17]=2)[CH:10]=[C:11]([Cl:12])[C:6]=1[OH:5]

Participants

3

Reactant 2

HCID 8029FuranHCID 20027393HCID 20027393, compound

Product 1

HCID 20027406HCID 20027406, compoundYield 52%

Procedure

2,6-Dichloro-4-(2-furanyl)phenol [IV; R1 =2-Cl, R2 =6-Cl, Het=2-furanyl] was prepared from 2,6-dichloro-4-iodophenyl trimethylsilyl ether and furan according to the procedure of Example 1(b), and was obtained in 52% yield as a light brown solid, m.p. 68-70° C.

Workup

  1. customwas obtained in 52% yield as a light brown solid, m.p. 68-70° C.

Sources & evidence

ORD record
ord-d4cd48d779ae4e329d1484a5193b2f7b
Source dataset
uspto-grants-1989_08
Patent number
US04857539

Reaction notes

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