HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14989153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Bromo-2-butanone | HCID 13156 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14989153 | HCID 14989153 | — |
Reaction Steps
The thiol of Example 2 (7.1 g, 0.03 M) was reacted with 1-bromo-2-butanone (5 g) and triethylamine (4.2 ml) in ethyl ether (25 ml) by the method of Example 8 to give the title compound, m.p. ca. 55°-57° C. Analysis calc. for C18H28O2S (308.48)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857558 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-c1778302105f495fa562af43ade3b552 |
| Source note | uspto-grants-1989_08 |