HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14989154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | 2-Pentanone, 5-chloro- | HCID 79993 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14989154 | HCID 14989154 | — |
Reaction Steps
The thiol of Example 2 (5.0 g, 0.021 M) was reacted with 5-chloro-2-pentanone (2.87 ml) and triethylamine (3.0 ml) in ethyl ether (50 ml) by the method of Example 8 to give the title compound, m.p. ca. 65°-67° C. Analysis calc. for C19H30O2S(322.49):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857558 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-c62f96fbf1d84b8f964a8cce41d4a90f |
| Source note | uspto-grants-1989_08 |