HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 10361139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Bromopropanoyl chloride | HCID 97980 | — |
| Reactant | 2-[(2-Methoxyphenoxy)methyl]-1,3-thiazolidine | HCID 3025454 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10361139 | HCID 10361139 | — |
Reaction Steps
α-Bromopropionyl chloride (0.97 ml) in methylene chloride (15 ml) is added dropwise to a mixture of 2-(o-methoxyphenoxy)methyl-thiazolidine (2 g) and triethylamine (1.35 ml) in CH2Cl2 (30 ml) at 0°-5° C. After 1 hour, the mixture is washed with water and the usual work-up gives 3-α-bromopropionyl-2-(o-methoxyphenoxy)methyl-thiazolidine as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857643 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-cf733f7ba06a4092ab146fdbb9df768f |
| Source note | uspto-grants-1989_08 |