HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | Acrylamide, N-cyclohexyl- | HCID 137811 | — |
| Reactant | 2-(4-Nitrophenyl)prop-2-enoic acid | HCID 13278029 | — |
| Product | 4-Aza-4-cyclohexyl-2-(4-nitrophenyl)-1,6-heptadiene-3,5-dione | HCID 20027806 | — |
Reaction Steps
The title compound is prepared analogously to Example 1c starting from 40.5 g of α-(4-nitrophenyl)-acrylic acid, 26.7 g of oxalyl chloride and 26.8 g of N-cyclohexylacrylamide. Melting point 73°-74° (from hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857660 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-b6c2dad9ba3a415991dc17579c19601a |
| Source note | uspto-grants-1989_08 |