Hydrazine → HCID 20026195, compound

Participants

Reaction Steps

To a solution of 0.22 mol. hydrazine in 100 ml. chloroform at -10° C. was added 0.1 mol of 2,3,6-trichlorobenzoyl chloride. The mixture was stirred at ambient temperature for 2 hours, filtered, and the filtrate evaporated in vacuo. The residue was crystallized from methanol and water, then recrystallized from chloroform and hexane to obtain the titled product.

Provenance & Evidence