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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1722929Generated: October 31, 2026

2,6-Dichloroaniline → HCID 14255125, compound

https://huagongshe.com/reaction/1722929

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2,6-DichloroanilineHCID 11846—
Reactant1-Acetyl-5-amino-1H-1,2,4-triazole-3-sulfonyl chlorideHCID 14255123—
SolventPyridineHCID 1049—
ProductHCID 14255125HCID 14255125—

Reaction Conditions

Temperature60 °C

Reaction Steps

42.63 g (0.26 mol) 2,6-dichloroaniline in 350 ml pyridine was treated with 54 g (0.24 mol) of 1-acetyl-5-amino-1,2,4-triazole-3-sulphonyl chloride and stirred at 60° C. for 12 hours. After cooling, the crystals were separated, washed with a small amount of pyridine and ether and dried in vacuo.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04859231
Source datasetuspto-grants-1989_08
ORD IDord-1483a166394c4418929d1bf60c27169b
Source noteuspto-grants-1989_08