HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenacyl bromide → HCID 20026006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenacyl bromide | HCID 6259 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-methyl-6-trifluoromethyl-3-(4-chloro-2-fluoro-5-hydroxyphenyl)-2,4(1H,3H)-pyrimidinedione | HCID 11267757 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20026006 | HCID 20026006 | — |
Reaction Steps
using 3-(4-chloro-2-fluoro-5-hydroxyphenyl)-1-methyl-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione with α-bromoacetophenone and sodium hydride in dimethylformamide there is obtained 3-[4-chloro-2-fluoro-5-(phenacyloxy)-phenyl]-1-methyl-6 -trifluoromethyl-2,4(1H,3H)-pyrimidinedione, m.p. 152°-153° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859229 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-1b3524c30d194bb0b3a73dbddf0b2122 |
| Source note | uspto-grants-1989_08 |