HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl chloroformate → Methyl 4-[6-(butoxycarbonyl)aminobenzimidazol-1-ylmethyl]-3-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | Methyl 4-(6-aminobenzimidazol-1-ylmethyl)-3-methoxybenzoate | HCID 14763098 | — |
| Product | Methyl 4-[6-(butoxycarbonyl)aminobenzimidazol-1-ylmethyl]-3-methoxybenzoate | HCID 23365847 | 34% |
Reaction Steps
Using a similar procedure to that described in Example 35, but using butyl chloroformate and (J), the title compound was obtained as a solid in 34% yield; partial NMR: 0.9(t,3H, CH3CH2), 1.4(m,2H, CH3CH2), 1.6(m,2H, CH2O), 4.1(t,2H, CH2O).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859692 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-35b9144a19cc44cea3edf93b5ecdbd37 |
| Source note | uspto-grants-1989_08 |