Cyanamide → HCID 178457522, compound

HRID 1723252Notes

Reaction equation

HRID 1723252 reaction equation
[CH2:1]([N:4]=[C:5]=[N:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH:2]=[CH2:3].[N:13]#[C:14][NH2:15]>>[CH2:1]([NH:4][C:5]([NH:15][C:14]#[N:13])=[N:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 9864CyanamideHCID 20026806HCID 20026806, compound

Product 1

HCID 178457522HCID 178457522, compound

Procedure

0.6 g of N-allyl-N'-phenylcarbodiimide in 8 ml of 1,2-dichloromethane is reacted with 0.17 g cyanamide and the reaction mixture is worked up as described in Example 4. Recrystallisation from diethyl ether yields a colourless crystalline product which melts at 99.5°-100.5° C.

Workup

  1. customRecrystallisation from diethyl ether
  2. customyields a colourless crystalline product which melts at 99.5°-100.5° C.

Sources & evidence

ORD record
ord-a430828b7caa4ebca6d99ce75ba91cf6
Source dataset
uspto-grants-1989_08
Patent number
US04859761

Reaction notes

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