HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoroaniline → HCID 3265055, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoroaniline | HCID 9584 | — |
| Reactant | 1,3-Cyclohexanedione | HCID 10434 | — |
| Product | HCID 3265055 | HCID 3265055 | 80.9% |
Reaction Steps
2-Fluoroaniline (10 g) and cyclohexane-1,3-dione (10 g) were heated together under nitrogen at 120° for 1 h. The cooled mixture was triturated with ether and filtered to give the title compound (14.8 g), m.p. 116°-118°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859662 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-e01f602fc3a5447097d8424415fafa82 |
| Source note | uspto-grants-1989_08 |