HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 2-n-Nonyl-1,3-dioxolane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Product | 2-n-Nonyl-1,3-dioxolane | HCID 78056 | 77.4% |
Reaction Steps
Following example I from 78.77 g of decylaldehyde (0.5 mole), 37.22 g (0.6 mole) of ethyleneglycol, 0.5 g of p-toluenesulfonic acid in 100 ml toluene there is obtained 78 g (77.4%) of a colorless product; b.p. 80°-81° C./0.5 mm. nD20 =1.4392.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861764 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-bc96902b02724573805859e5a6169fce |
| Source note | uspto-grants-1989_08 |