HuagongsheHuagongshe Chemistry Print Report · For research reference only
30336-13-1 → 5-(Furan-2-yl)pentan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 30336-13-1 | HCID 12594357 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-(Furan-2-yl)pentan-1-ol | HCID 13296436 | 92.8% |
Reaction Steps
5-(2-Furanyl)pentanoic acid (60.4 g) was reduced with 13.7 g of lithium aluminum hydride in 400 ml of tetrahydrofuran, heated at reflux for about 16 hours. The product was isolated and purified by distillation to give 51.4 g of 5-(2-furanyl)pentanol, b.p. 70°-73° C. (0.1 mm).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861791 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-b38da89f3e814d04ac746fa263734087 |
| Source note | uspto-grants-1989_08 |