Dibutylamine → (E)-2-[2-(4-Dibutylaminopropoxyphenyl)ethenyl]-6-methoxybenzoxazole

Participants

Reaction Steps

Reaction of this product (2.4 g, 6.9 mmol) with dibutylamine produced 0.20 g (8% yield) of the named compound as the HCl salt, mp 151°-152° C. IR(KBr): 1600 cm-1. MS: 437(MH+). 1H NMR (CDCl3): δ 8.31-6.91 (m, 9H), 4.18 (t, J=5.1 Hz, 2H), 3.91 (s, 3H), 3.09 (m, 4H), 2.67-0.82 (m, 18H).

Provenance & Evidence