Dibutylamine → HCID 20025797, compound

HRID 1723517Notes

Reaction equation

[CH2:1]([NH:5][CH2:6][CH2:7][CH2:8][CH3:9])[CH2:2][CH2:3][CH3:4].Cl[CH2:11][CH2:12][CH2:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1/[CH:21]=[CH:22]/[C:23]1[S:24][C:25]2[CH:31]=[CH:30][CH:29]=[CH:28][C:26]=2[N:27]=1>>[CH2:1]([N:5]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:11][CH2:12][CH2:13][O:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1/[CH:21]=[CH:22]/[C:23]1[S:24][C:25]2[CH:31]=[CH:30][CH:29]=[CH:28][C:26]=2[N:27]=1)[CH2:2][CH2:3][CH3:4]

Participants

Reactant 2

HCID 8148Dibutylamine

HCID 20025825HCID 20025825, compound

Product 1

HCID 20025797HCID 20025797, compoundYield 34%

Procedure

Reaction of this product (3.0 g, 9.1 mmol) with dibutylamine produced 1.5 g (34% yield) of the title compound as the HCl salt, mp 182°-184° C. IR(KBr): 3400, 1600 cm-1. MS: 422(M+). 1H NMR (CDCl3): δ 8.28-6.87 (m 10H), 4.19 (t, J=5.3 Hz, 2H), 3.74-2.93 (m, 6H), 2.51-0.82 (m, 16H).

Sources & evidence

ORD record: ord-f4115384177b406e9dd543d0ab4c9da4
Source dataset: uspto-grants-1989_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04861897

Reaction notes

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