2-Methylbenzothiazole → HCID 14146369, compound

Participants

Reaction Steps

The named compound was prepared as described in Example 17 starting with 4-chloroethoxybenzaldehyde (4.0 g, 22 mmol) and using 2-methylbenzothiazole in place of 2-methylbenzoxazole to give (E)-2-[2-(4-chloroethoxyphenyl)ethenyl]benzothiazole (G) (7.6 g, 90% yield) as a yellow solid, mp 92°-94° C. 1H NMR (CDCl3): δ 8.09-6.85 (m, 10H), 4.23 (t, J=5.2 Hz, 2H), 3.81 (t, J=5.2 Hz, 2H).

Provenance & Evidence