Dipropylamine → HCID 20025791, compound

HRID 1723525Notes

Reaction equation

[CH2:1]([NH:4][CH2:5][CH2:6][CH3:7])[CH2:2][CH3:3].Cl[CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1/[CH:20]=[CH:21]/[C:22]1[S:23][C:24]2[CH:30]=[CH:29][CH:28]=[CH:27][C:25]=2[N:26]=1>>[CH2:1]([N:4]([CH2:5][CH2:6][CH3:7])[CH2:9][CH2:10][CH2:11][CH2:12][O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1/[CH:20]=[CH:21]/[C:22]1[S:23][C:24]2[CH:30]=[CH:29][CH:28]=[CH:27][C:25]=2[N:26]=1)[CH2:2][CH3:3]

Participants

Reactant 2

HCID 8902Dipropylamine

HCID 20025798HCID 20025798, compound

Product 1

HCID 20025791HCID 20025791, compoundYield 35%

Procedure

Reaction of this product (5.0 g, 14.5 mmol) with dipropylamine produced 2.1 g (35% yield) of the named compound as the HCl salt, mp 155°-156° C. IR(KBr): 3400, 1600 cm-1. MS: 409(MH+). 1H NMR (CD3OD): δ 8.19-6.99 (m, 10H), 4.10 (t, J=5.2 Hz, 2H), 3.12(m, 6H), 1.85(m, 8H), 1.02 (m, 6H).

Sources & evidence

ORD record: ord-e15ae4b72b1c4bc89ec8fb7fa9b4b461
Source dataset: uspto-grants-1989_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04861897

Reaction notes

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