HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → HCID 53905861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 13339540 | HCID 13339540 | — |
| Solvent | Diethylether pentane | HCID 21877078 | — |
| Product | HCID 53905861 | HCID 53905861 | — |
Reaction Steps
By the procedure of Example A1, but using 13:7 hexane:ethyl acetate and then 3:7 hexane:ethyl acetate as eluant and ether/pentane for crystallization, 1-(3-fluorophenyl)-2(1H,3H)-indolone (0.80 g, 3.5 mmoles) was converted to title product, 0.53 g, m.p. 87°-88.5°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861880 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-ad74b3c7571b4bf190a5edc29226e30a |
| Source note | uspto-grants-1989_08 |