HCID 53970952, compound → 2H-Indol-2-one, 3-[(dimethylamino)methylene]-1,3-dihydro-, (Z)-

HRID 1723541Notes

Reaction equation

HRID 1723541 reaction equation
Cl[C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][C:6](=[O:11])[C:5]2=[CH:12][N:13]([CH3:15])[CH3:14].ClC1C=C2C(=CC=1)NC(=O)C2.COC(OC)N(C)C>>[CH3:15][N:13]([CH:12]=[C:5]1[C:4]2[C:8](=[CH:9][CH:10]=[CH:2][CH:3]=2)[NH:7][C:6]1=[O:11])[CH3:14]

Participants

3

Reactant 2

HCID 53970952HCID 53970952, compoundHCID 131713911HCID 131713911, compound

Product 1

HCID 30289742H-Indol-2-one, 3-[(dimethylamino)methylene]-1,3-dihydro-, (Z)-

Procedure

A17. 5-Chloro-3-(dimethylaminomethylene)-2(1H,3H)-indolone; 5-chlorooxindole/dimethylformamide dimethylacetal; 67%; 204°-206°.

Workup

  1. custom204°-206°

Sources & evidence

ORD record
ord-9808e017afbf4beca2ca8ffc1849bc97
Source dataset
uspto-grants-1989_08
Patent number
US04861880

Reaction notes

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