4-(4-Chlorophenyl)-1,2,3,6-tetrahydropyridinium chloride → HCID 11524741, compound

HRID 1723636Notes

Reaction equation

HRID 1723636 reaction equation
[N:1]1([C:7]2[CH:15]=[CH:14][C:13]([N+:16]([O-:18])=[O:17])=[CH:12][C:8]=2[C:9](Cl)=[O:10])[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.Cl.[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([C:27]2[CH2:28][CH2:29][NH:30][CH2:31][CH:32]=2)=[CH:23][CH:22]=1>>[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([C:27]2[CH2:32][CH2:31][N:30]([C:9]([C:8]3[CH:12]=[C:13]([N+:16]([O-:18])=[O:17])[CH:14]=[CH:15][C:7]=3[N:1]3[CH2:6][CH2:5][O:4][CH2:3][CH2:2]3)=[O:10])[CH2:29][CH:28]=2)=[CH:23][CH:22]=1

Participants

3

Reactant 2

HCID 27236124-(4-Chlorophenyl)-1,2,3,6-tetrahydropyridinium chlorideHCID 172741532-Morpholin-4-yl-5-nitro-benzoyl chloride

Product 1

HCID 11524741HCID 11524741, compound

Procedure

According to the procedure described for the synthesis of example 1, the title compound has been synthesized from 2-morpholin-4-yl-5-nitro-benzoyl chloride and 4-(4-Chloro-phenyl)-1,2,3,6-tetrahydro-pyridine hydrochloride (commercial). MS (m/e): 428.1 (MH+, 100%)

Workup

  1. customdescribed for the synthesis of example 1

Sources & evidence

ORD record
ord-dd02f8d55c4346c2bc68904933abdfa5
Source dataset
uspto-grants-2009_02
Patent number
US07485637B2

Reaction notes

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